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Supervisors: Dott.ssa Emilia Bramanti, prof.ssa Stefania Giannarelli

Title: Quantification and monitoring of inorganic compounds relevant for environmental and health risk assessment

Abstract: The key-point of my research activity is the quantitation, speciation and monitoring of relevant inorganic contaminants by inductively coupled plasma mass spectrometry (ICP-MS), a technique characterized by greater speed and sensitivity, and by atomic fluorescence spectrometry (AFS), an alternative and low-cost technique compared to ICP-MS.
I am participating in a European project aimed to demonstrate the application of ecological and sustainable strategies for the control of bacterial infections in plants replacing traditional products based on copper. My participation to the project includes the speciation of copper and quantification of phytohormones in plants by HPLC-ICP-MS and HPLC-DAD-Fluorescence, respectively.
I am also developing a method for the photochemical vapor generation of organo-compounds of mercury, selenium and arsenic and their determination with AFS.

Publications:
•    Ammazzini, S., Onor, M., Pagliano, E., Mester, Z., Campanella, B., Pitzalis, E., D’Ulivo, A. (2015) Journal of Chromatography A 1400 PP. 124 – 130
•    Campanella, B., Onor, M., Biancalana, L., D'Ulivo, A., Bramanti, E. (2015) Analytical Biochemistry 483 PP. 27 – 33
•    de Quadros, D., Campanella, B., Onor, M., Bramanti, E., Borges, D., D’Ulivo, A. (2014) Spectrochimica Acta Part B: Atomic Spectroscopy 101 PP. 312 – 319
•    Campanella, B., Bramanti, E. (2014) Analyst 139 (17) PP. 4124-4153
•    Campanella, B., Onor, M., Ferrari, C., D'Ulivo, A., Bramanti, E. (2014) Analytica Chimica Acta 843 PP. 1 – 6
•    Campanella, B., Onor, M., D'Ulivo, A., Giannarelli, S., Bramanti, E. (2014) Analytical Chemistry 86 (4) PP. 2251 – 2256
•    Campanella, B., Rivera, J.G., Ferrari, C., Biagi, S., Onor, M., D'Ulivo, A., Bramanti, E. (2013) Analytical Chemistry 85 (24) PP. 12152 – 12157
•    Campanella, B., Onor, M., Mascherpa, M.C., D'Ulivo, A., Ferrari, C., Bramanti, E. (2013) Analytica Chimica Acta 804 PP. 66 – 69

Oral communications at congress:
"Proteomics low-cost: study of proteins with probe labelling mercurial coupled to atomic fluorescence spectrometry with chemical vapor generation (CVG-AFS)".
Campanella, B., Rivera, J.G., Ferrari, C., Biagi, S., Onor, M., D'Ulivo, A., Bramanti, E.
XXIV Congresso della Divisione di Chimica Analitica della Società Chimica Italiana, Sestri Levante, Sep 2013
[Book of abstract pg. 65]

Poster communications at congress:
Title: “Rapid clean-up strategy based on molecularly imprinted polymers for the determination of 3- indoleacetic acid in plant extracts”.
B. Campanella, E. Pulidori, M. Onor, S. Tegli, P. Bogani, M. Cerboneschi,
E. Passaglia, A. D’Ulivo, E. Bramanti
XXV Congresso della Divisione di Chimica Analitica della Società Chimica Italiana, Sestri Levante, Sep 2015
[Book of abstract pg. 56]

Title: “Hyphenated Techniques - protein determination and characterization”.
E. Bramanti, B. Campanella, M. Onor, A. D’Ulivo
XXXIX Colloquium Spectroscopicum Internationale” (Figueira da Foz, Portugal), Aug 2015
[Book of abstract pg. 30]

Title: “Photochemical vapor generation of selenium(IV) and arsenic(III) with commercial and homemade UV lamps”.
A. Menciassi, B. Campanella, M. Onor, A. D’Ulivo, E. Bramanti, C. Ferrari, I. Longo
XXXIX Colloquium Spectroscopicum Internationale” (Figueira da Foz, Portugal), Aug 2015
[Book of abstract pg. 123]

Title: “Thallium determination in contaminated water and biological samples: a population-based case–control study in Valdicastello Carducci and Pietrasanta (Lucca, Italy)”.
E. Bramanti, M. Onor, B. Campanella, A. D’Ulivo, S. Biagi, G. Rossi, O. Curzio, R. Giannecchini, M. D’Orazio, R. Petrini
XXXIX Colloquium Spectroscopicum Internationale” (Figueira da Foz, Portugal), Aug 2015
[Book of abstract pg. 254]

Title: “Determination of carboxylic acids in biological matrices by GC/MS following single-step aqueous derivatization with triethyloxonium tetrafluoroborate”.
D. Ferraro, M. Onor, B. Campanella, S. Tegli, E. Bramanti, S. Giannarelli,
A. D’Ulivo and E. Pagliano
XXXIX Colloquium Spectroscopicum Internationale” (Figueira da Foz, Portugal), Aug 2015
[Book of abstract pg. 277]

Title: “Effect of the use of copper compounds on plants for the control of bacterial diseases”.
B. Campanella, M. Onor, A. D’Ulivo, S. Tegli, P. Bogani, M. Cerboneschi, E. Bramanti
XXXIX Colloquium Spectroscopicum Internationale” (Figueira da Foz, Portugal), Aug 2015
[Book of abstract pg. 320]

Title: “Low-cost proteomics: study of proteins with probe labeling mercurial coupled to atomic fluorescence spectrometry with chemical vapor generation (CVG-AFS)”.
Campanella, B., Rivera, J.G., Ferrari, C., Biagi, S., Onor, M., D'Ulivo, A., Bramanti, E.
XXXVIII Colloquium Spectroscopicum Internationale” (Tromsø, Norvegia), Jun 2013
[Book of abstract pg. 19]